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The study of longifolene by two‐dimensional NMR spectroscopy

The study of longifolene by two‐dimensional NMR spectroscopy The complete assignment of the 13C NMR spectrum of longifolene was achieved from double quantum coherence measurements, while combined evaluation of a 1H13C heteronuclear chemical shift correlation diagram and a homonuclear 1H J‐resolved diagram provided all proton chemical shifts. Conformational information on the seven‐membered ring of the tricyclic sesquiterpene was obtained from proton chemical shift considerations. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Magnetic Resonance in Chemistry Wiley

The study of longifolene by two‐dimensional NMR spectroscopy

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References (16)

Publisher
Wiley
Copyright
Copyright © 1984 Wiley Subscription Services, Inc., A Wiley Company
ISSN
0749-1581
eISSN
1097-458X
DOI
10.1002/mrc.1270220711
Publisher site
See Article on Publisher Site

Abstract

The complete assignment of the 13C NMR spectrum of longifolene was achieved from double quantum coherence measurements, while combined evaluation of a 1H13C heteronuclear chemical shift correlation diagram and a homonuclear 1H J‐resolved diagram provided all proton chemical shifts. Conformational information on the seven‐membered ring of the tricyclic sesquiterpene was obtained from proton chemical shift considerations.

Journal

Magnetic Resonance in ChemistryWiley

Published: Jul 1, 1984

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