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Dynamic Small‐Angle X‐ray Scattering System using an Imaging Plate

Dynamic Small‐Angle X‐ray Scattering System using an Imaging Plate A synchrotron‐radiation dynamic small‐angle X‐ray scattering (Synchrotron Radiation‐DSAXS) system using an imaging plate has been developed at the Photon Factory, National Laboratory for High Energy Physics, Japan, in collaboration with the Department of Polymer Chemistry, Kyoto University, Japan, for studying the dynamic response of mesoscopic structures in polymers to applied mechanical stimuli. Small‐angle X‐ray scattering patterns of 100 × 100 mm2 have been successively recorded on a 400 × 200 mm2 stage‐mounted imaging plate with a minimum time interval of 0.5 s. X‐ray data are simultaneously obtained with stress and strain measurements on specimens subjected to a mechanical deformation. The performance of the DSAXS system is demonstrated along with some experimental results concerning the dynamic deformation of a b.c.c. lattice with paracrystalline distortion in a co‐polymer having spherical microdomains under a large oscillatory shear deformation. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Journal of Synchrotron Radiation Wiley

Dynamic Small‐Angle X‐ray Scattering System using an Imaging Plate

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Publisher
Wiley
Copyright
Copyright © 1996 Wiley Subscription Services, Inc., A Wiley Company
ISSN
1600-5775
eISSN
1600-5775
DOI
10.1107/S0909049596006498
pmid
16702683
Publisher site
See Article on Publisher Site

Abstract

A synchrotron‐radiation dynamic small‐angle X‐ray scattering (Synchrotron Radiation‐DSAXS) system using an imaging plate has been developed at the Photon Factory, National Laboratory for High Energy Physics, Japan, in collaboration with the Department of Polymer Chemistry, Kyoto University, Japan, for studying the dynamic response of mesoscopic structures in polymers to applied mechanical stimuli. Small‐angle X‐ray scattering patterns of 100 × 100 mm2 have been successively recorded on a 400 × 200 mm2 stage‐mounted imaging plate with a minimum time interval of 0.5 s. X‐ray data are simultaneously obtained with stress and strain measurements on specimens subjected to a mechanical deformation. The performance of the DSAXS system is demonstrated along with some experimental results concerning the dynamic deformation of a b.c.c. lattice with paracrystalline distortion in a co‐polymer having spherical microdomains under a large oscillatory shear deformation.

Journal

Journal of Synchrotron RadiationWiley

Published: Sep 1, 1996

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