Heterometallic complex [K3Y(Cat36)3(Dme)4] (I) or binuclear complex [Y2(Cat36)3(Dme)3] · Dme (II · Dme) is synthesized, depending on the reactant ratio, by the reaction of YCl3 with 3,6-bis(tertbutylcatecholate) potassium salt (K2Cat36) in 1,2-dimethoxyethane (Dme). Both complexes are characterized by single-crystal X-ray diffraction analysis (CIF files CCDC nos. 1527929 (I) and 1527930 (II)) and 1H and 13C NMR spectroscopy.
Russian Journal of Coordination Chemistry – Springer Journals
Published: Aug 19, 2017
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