Res Chem Intermed (2017) 43:3237–3249 DOI 10.1007/s11164-016-2822-2 Visible light motivated synthesis of polyhydroquinoline derivatives using CdS nanowires 1 1 • • Rajkumar R. Harale Praveen V. Shitre 1 1 Bhaskar R. Sathe Murlidhar S. Shingare Received: 5 October 2016 / Accepted: 25 November 2016 / Published online: 5 December 2016 Springer Science+Business Media Dordrecht 2016 Abstract In this article, we report the synthesis of one-dimensional cadmium sulphide nanowires (CdS NWs) by chemical synthesis approach. These as-synthesized materials were characterized by ultraviolet–visible spectroscopy, X-ray diffraction, scanning electron microscopy with energy dispersive spectroscopy, and transmission electron microscopy analysis. These nanowires have an average diameter of *20 nm and length up to several micrometres. CdS NWs are highly stability and are found to be a very efﬁcient recyclable/reusable (minimum four times without any signiﬁcant loss) photo- catalyst for polyhydroquinoline synthesis under visible light (Halogen lamp, 70 W) at room temperature. This system offers a mild, efﬁcient, and highly economical alternative to the existing protocols in its catalytic activity under visible light irradiation (k C 420 nm). These ﬁndings will open up new opportunities for developing low-cost efﬁcient photocatalyst synthesis of value added intermediates. & Murlidhar S. Shingare email@example.com Bhaskar R. Sathe firstname.lastname@example.org
Research on Chemical Intermediates – Springer Journals
Published: Dec 5, 2016
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