Two mononuclear complexes, [M(o-ClPhH2IDC)2(H2O)2] · 4H2O (o-ClPhH2IDC = 2-(o-chlorophenyl)-1H-imidazole-4,5-dicarboxylicacid; M = Co(I) and Mn(II)), have been solvothermally synthe-sized and structurally characterized by single crystal X-ray diffraction (CIF files CCDC nos. 1036900 (I) and 1036899 (II)), elemental analyses, IR spectroscopy, and powder X-ray diffractionIn both supramolecules, the [Co(o-ClPhH2IDC)2(H2O)2] or [Mn(o-ClPhH2IDC)2(H2O)2] units are joined through the π–π interactions and intermolecular hydrogen bonds to form the 3D solid-state architectures. Their thermal properties under are have been investigated as well.
Russian Journal of Coordination Chemistry – Springer Journals
Published: Aug 1, 2015
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