A series of framework phosphates with varied ratio of cations Na5-2x B x IIZr(PO4)3, BII = Mg, Ca, Sr, Ba (0 ≤ x ≤ 2) and Na5-3x Fe x Zr(PO4)3 (0 ≤ x ≤ 1.33) were synthesized and studied under heating. The coefficients of thermal expansion along crystal axes α a and α c were calculated, and their dependences on the cationic composition (nature and concentration) and on the occupancy of out-of-framework structural positions were established.
Russian Journal of Applied Chemistry – Springer Journals
Published: Sep 30, 2004
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