Thermal behavior of titanium tetrabutylate and niobium pentapropylate in a wide temperature range under static conditions was studied with a membrane zero-gage. The vapor pressure under conditions when vaporization is not complicated by other processes was determined. The enthalpy and entropy of vaporization were calculated. The mechanism of thermolysis of Ti(OBu)4 and Nb(OPr)5 was studied.
Russian Journal of Applied Chemistry – Springer Journals
Published: Oct 13, 2004
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