The effects of the crystallization rate of the mesoporous TiO2 on the stability of the mesoporous structure after reflux

The effects of the crystallization rate of the mesoporous TiO2 on the stability of the mesoporous... A simple synthetic method was employed to prepare mesoporous titania with anatase crystalline walls and high photocatalytic activity. The properties and structures of mesoporous titania were characterized by means of low angle and wide angle X-ray diffraction (XRD), Fourier transform (FT)-IR spectra, transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and N2 adsorption–desorption. The characteristic results clearly show that crystallization rate of the mesoporous titania affects the stability of the mesoporous structure after reflux, and that the anatase crystal in the mesoporous wall of mesoporous titania can stabilize the mesoporous structure. The photocatalytic activity of titania powder was evaluated from an analysis of the photodegradation of methyl orange under UV irradiation. The results indicate that the titania powder with mesoporous structure shows the highest photocatalytic activity. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Research on Chemical Intermediates Springer Journals

The effects of the crystallization rate of the mesoporous TiO2 on the stability of the mesoporous structure after reflux

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Publisher
Springer Journals
Copyright
Copyright © 2009 by Springer Science+Business Media B.V.
Subject
Chemistry; Inorganic Chemistry ; Physical Chemistry ; Catalysis
ISSN
0922-6168
eISSN
1568-5675
D.O.I.
10.1007/s11164-009-0095-8
Publisher site
See Article on Publisher Site

Abstract

A simple synthetic method was employed to prepare mesoporous titania with anatase crystalline walls and high photocatalytic activity. The properties and structures of mesoporous titania were characterized by means of low angle and wide angle X-ray diffraction (XRD), Fourier transform (FT)-IR spectra, transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and N2 adsorption–desorption. The characteristic results clearly show that crystallization rate of the mesoporous titania affects the stability of the mesoporous structure after reflux, and that the anatase crystal in the mesoporous wall of mesoporous titania can stabilize the mesoporous structure. The photocatalytic activity of titania powder was evaluated from an analysis of the photodegradation of methyl orange under UV irradiation. The results indicate that the titania powder with mesoporous structure shows the highest photocatalytic activity.

Journal

Research on Chemical IntermediatesSpringer Journals

Published: Dec 8, 2009

References

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