The catalysis, synthesis and characterization of ferrocenylchalcone

The catalysis, synthesis and characterization of ferrocenylchalcone Eight kinds of ferrocenylchalcone derivatives were synthesized by the reaction of acetylferrocene and aromatic aldehyde using solid as catalyst in the experiment. The influrence of the catalysts, the raw material molar ratios and reaction times on the yield of ferrocenylchalcone derivatives are discussed. The optimal conditions of synthesis reaction have been selected: the catalyst was KF/Al2O3, n(acetyl ferrocene)/n(formal dehyde) = 1:1.2. The structures of the products were characterized by melting point test, IR, 1HNMR, 13CNMR and elemental analysis. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Research on Chemical Intermediates Springer Journals

The catalysis, synthesis and characterization of ferrocenylchalcone

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Publisher
Springer Netherlands
Copyright
Copyright © 2012 by Springer Science+Business Media B.V.
Subject
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
ISSN
0922-6168
eISSN
1568-5675
D.O.I.
10.1007/s11164-012-0810-8
Publisher site
See Article on Publisher Site

Abstract

Eight kinds of ferrocenylchalcone derivatives were synthesized by the reaction of acetylferrocene and aromatic aldehyde using solid as catalyst in the experiment. The influrence of the catalysts, the raw material molar ratios and reaction times on the yield of ferrocenylchalcone derivatives are discussed. The optimal conditions of synthesis reaction have been selected: the catalyst was KF/Al2O3, n(acetyl ferrocene)/n(formal dehyde) = 1:1.2. The structures of the products were characterized by melting point test, IR, 1HNMR, 13CNMR and elemental analysis.

Journal

Research on Chemical IntermediatesSpringer Journals

Published: Sep 30, 2012

References

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