Synthesis of molybdenum disulfide particles by aerosol-assisted chemical vapor deposition

Synthesis of molybdenum disulfide particles by aerosol-assisted chemical vapor deposition It was shown that dimethylformamide can be, in principle, used as a solvent of ammonium thiomolybdate for obtaining molybdenum disulfide particles by the aerosol-assisted chemical vapor deposition method. IR Fourier spectroscopy was used to examine (NH4)2MoS4–C3H7NO liquid solutions and the thermal stability of dimethylformamide and ammonium thiomolybdate vapors. It was demonstrated that pyrolysis at temperatures of 700–900°C yields spherical molybdenum disulfide microparticles with average diameters in the range 0.6–1 µm and “onion” structure. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Russian Journal of Applied Chemistry Springer Journals

Synthesis of molybdenum disulfide particles by aerosol-assisted chemical vapor deposition

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Publisher
Springer Journals
Copyright
Copyright © 2016 by Pleiades Publishing, Ltd.
Subject
Chemistry; Chemistry/Food Science, general; Industrial Chemistry/Chemical Engineering
ISSN
1070-4272
eISSN
1608-3296
D.O.I.
10.1134/S1070427216050050
Publisher site
See Article on Publisher Site

Abstract

It was shown that dimethylformamide can be, in principle, used as a solvent of ammonium thiomolybdate for obtaining molybdenum disulfide particles by the aerosol-assisted chemical vapor deposition method. IR Fourier spectroscopy was used to examine (NH4)2MoS4–C3H7NO liquid solutions and the thermal stability of dimethylformamide and ammonium thiomolybdate vapors. It was demonstrated that pyrolysis at temperatures of 700–900°C yields spherical molybdenum disulfide microparticles with average diameters in the range 0.6–1 µm and “onion” structure.

Journal

Russian Journal of Applied ChemistrySpringer Journals

Published: Aug 12, 2016

References

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