Addition reactions of ethane-1,2-diol, propane-1,3-diol, and butane-1,4-diol to bicyclo[2,2,1]hept-2-ene in the presence of a catalyst BF3 OEt2 were studied for deriving reactive monomer, therewith bicyclo[2.2.1] hept-2-oxyalcanols with a yield of 91.2–96.0% were synthesized. In the second stage esterification of the obtained bicyclo[2.2.1]hept-2-oxyalkanols was conducted with acrylic acid in the presence of a catalyst of KU-2-8 H grade and acrylates was also derived with a yield of 87.5–93.0%, which are reactive monomers for synthesis of polymeric glassy products.
Russian Journal of Applied Chemistry – Springer Journals
Published: Jan 23, 2015
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