Higher empty and endohedral gadolinium metallofullerenes were prepared by electric arc synthesis, isolated, and separated chromatographically to high degree of purity (99 wt %). The samples obtained were characterized by chromatography, optical spectroscopy, and mass spectrometry. According to small-angle neutron scattering data, the endohedral metallofullerenes in o-xylene form a molecular solution in which the molecules interact to form molecular pairs.
Russian Journal of Applied Chemistry – Springer Journals
Published: May 13, 2014
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