Synthesis, crystal structure, and preliminary antibacterial activity of oxovanadium(V) complex with hydrazone ligand

Synthesis, crystal structure, and preliminary antibacterial activity of oxovanadium(V) complex... A new mononuclear oxovanadium(V) complex, [VOL(OMe)(MeOH)] (I), where L is the dianionic form of (1H-indol-3-yl)acetic acid [1-(2-hydroxynaphthalen-1-yl)methylidene]hydrazine, has been synthesized and characterized by physico-chemical methods and single crystal X-ray determination, (CIF file CCDC no. 858861). The complex crystallizes in the triclinic space group $$P\bar 1$$ with unit cell dimensions a = 10.117(1), b = 10.609(2), c = 11.454(2) Å, α = 99.228(2)°, β = 112.250(2)°, γ = 100.561(2)°, V = 1082.3(3)Å3, Z = 2, R 1 = 0.0512, and wR 2 = 0.1045. The V atom in complex I is in an octahedral coordination. Thermal analysis and preliminary antibacterial activity of complex I were studied. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Russian Journal of Coordination Chemistry Springer Journals

Synthesis, crystal structure, and preliminary antibacterial activity of oxovanadium(V) complex with hydrazone ligand

Loading next page...
 
/lp/springer_journal/synthesis-crystal-structure-and-preliminary-antibacterial-activity-of-zitMh08R0H
Publisher
Pleiades Publishing
Copyright
Copyright © 2015 by Pleiades Publishing, Ltd.
Subject
Chemistry; Physical Chemistry; Inorganic Chemistry
ISSN
1070-3284
eISSN
1608-3318
D.O.I.
10.1134/S1070328415070040
Publisher site
See Article on Publisher Site

Abstract

A new mononuclear oxovanadium(V) complex, [VOL(OMe)(MeOH)] (I), where L is the dianionic form of (1H-indol-3-yl)acetic acid [1-(2-hydroxynaphthalen-1-yl)methylidene]hydrazine, has been synthesized and characterized by physico-chemical methods and single crystal X-ray determination, (CIF file CCDC no. 858861). The complex crystallizes in the triclinic space group $$P\bar 1$$ with unit cell dimensions a = 10.117(1), b = 10.609(2), c = 11.454(2) Å, α = 99.228(2)°, β = 112.250(2)°, γ = 100.561(2)°, V = 1082.3(3)Å3, Z = 2, R 1 = 0.0512, and wR 2 = 0.1045. The V atom in complex I is in an octahedral coordination. Thermal analysis and preliminary antibacterial activity of complex I were studied.

Journal

Russian Journal of Coordination ChemistrySpringer Journals

Published: Jun 24, 2015

References

You’re reading a free preview. Subscribe to read the entire article.


DeepDyve is your
personal research library

It’s your single place to instantly
discover and read the research
that matters to you.

Enjoy affordable access to
over 12 million articles from more than
10,000 peer-reviewed journals.

All for just $49/month

Explore the DeepDyve Library

Unlimited reading

Read as many articles as you need. Full articles with original layout, charts and figures. Read online, from anywhere.

Stay up to date

Keep up with your field with Personalized Recommendations and Follow Journals to get automatic updates.

Organize your research

It’s easy to organize your research with our built-in tools.

Your journals are on DeepDyve

Read from thousands of the leading scholarly journals from SpringerNature, Elsevier, Wiley-Blackwell, Oxford University Press and more.

All the latest content is available, no embargo periods.

See the journals in your area

DeepDyve Freelancer

DeepDyve Pro

Price
FREE
$49/month

$360/year
Save searches from
Google Scholar,
PubMed
Create lists to
organize your research
Export lists, citations
Read DeepDyve articles
Abstract access only
Unlimited access to over
18 million full-text articles
Print
20 pages/month
PDF Discount
20% off