Synthesis, characterization, and photoluminescence properties of HgSe nanoparticles using a novel mercury precursor by the sonochemical method

Synthesis, characterization, and photoluminescence properties of HgSe nanoparticles using a novel... In this paper, we report the synthesis and characterization of novel mercury selenide (HgSe) nanoparticles by sonochemical method. The HgSe nanoparticles have been prepared using [N,N′-bis(salicylaldehydo)ethylenediamine] mercury(II), [Hg(salen)] complex, as a novel precursor. The effects of the different capping agents, such as sodium dodecyl-benzene-sulfonate, polyethylene glycol, and polyvinyl pyrrolidone on the particle size and morphology of the samples have been investigated. The effect of different parameters, such as: temperature, power of irradiation, and reducing agent were also examined. These nanoparticles were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, photoluminescence, X-ray energy dispersive spectroscopy, and Fourier transform infrared spectroscopy. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Research on Chemical Intermediates Springer Journals

Synthesis, characterization, and photoluminescence properties of HgSe nanoparticles using a novel mercury precursor by the sonochemical method

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Publisher
Springer Netherlands
Copyright
Copyright © 2014 by Springer Science+Business Media Dordrecht
Subject
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
ISSN
0922-6168
eISSN
1568-5675
D.O.I.
10.1007/s11164-014-1884-2
Publisher site
See Article on Publisher Site

Abstract

In this paper, we report the synthesis and characterization of novel mercury selenide (HgSe) nanoparticles by sonochemical method. The HgSe nanoparticles have been prepared using [N,N′-bis(salicylaldehydo)ethylenediamine] mercury(II), [Hg(salen)] complex, as a novel precursor. The effects of the different capping agents, such as sodium dodecyl-benzene-sulfonate, polyethylene glycol, and polyvinyl pyrrolidone on the particle size and morphology of the samples have been investigated. The effect of different parameters, such as: temperature, power of irradiation, and reducing agent were also examined. These nanoparticles were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, photoluminescence, X-ray energy dispersive spectroscopy, and Fourier transform infrared spectroscopy.

Journal

Research on Chemical IntermediatesSpringer Journals

Published: Dec 16, 2014

References

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