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Synthesis, characterization, and crystal structure of 6,7a-dichloro-3a-hydroxyoctahydro-1H-indene-2,5-diyl diacetates

Synthesis, characterization, and crystal structure of... The first syntheses and characterizations of 6,7a-dichloro-3a-hydroxyoctahydro-1H-indene-2,5-diyl diacetates were successfully obtained starting from indan-2-ol. Epoxidation of 2 was carried out using mCPBA in methylene chloride followed by acetylation using acetyl chloride to furnish the diacetates. The structures of all synthesized compounds were characterized by spectroscopic methods. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Journal of the Iranian Chemical Society Springer Journals

Synthesis, characterization, and crystal structure of 6,7a-dichloro-3a-hydroxyoctahydro-1H-indene-2,5-diyl diacetates

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Publisher
Springer Journals
Copyright
Copyright © 2018 by Iranian Chemical Society
Subject
Chemistry; Analytical Chemistry; Inorganic Chemistry; Physical Chemistry; Biochemistry, general; Organic Chemistry
ISSN
1735-207X
eISSN
1735-2428
DOI
10.1007/s13738-018-1394-z
Publisher site
See Article on Publisher Site

Abstract

The first syntheses and characterizations of 6,7a-dichloro-3a-hydroxyoctahydro-1H-indene-2,5-diyl diacetates were successfully obtained starting from indan-2-ol. Epoxidation of 2 was carried out using mCPBA in methylene chloride followed by acetylation using acetyl chloride to furnish the diacetates. The structures of all synthesized compounds were characterized by spectroscopic methods.

Journal

Journal of the Iranian Chemical Society – Springer Journals

Published: Jun 4, 2018

References