Substitutional solid solutions (Cu1−y Zn y )2(OH)PO4·xH2O (0 ≤ y ⩽ 0.26, x = 0.1−0.2), (Cu1−y Co y )2(OH)PO4·xH2O (0 ≤ y ≤ 0.10, x = 0.1−0.2), and (Cu1−y Ni y )2(OH)PO4·xH2O (0 ≤ y ≤ 0.08, x = 0.1−0.2) were synthesized. The unit cell parameters of the resulting phosphates were determined, and their IR absorption spectra were measured. The reactants were H3PO4 and mixtures of hydrous carbonates of the appropriate metals. Thermolysis of the solid solutions was examined with (Cu1−y Co y )2(OH)PO4·xH2O (0 ≤ y ≤ 0.10, x = 0.1−0.2) as an example.
Russian Journal of Applied Chemistry – Springer Journals
Published: Feb 1, 2010
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