Synthesis and properties of SnO prepared from ammoniacal and carbonate suspensions of tin(II) hydroxy compound under microwave radiation

Synthesis and properties of SnO prepared from ammoniacal and carbonate suspensions of tin(II)... SnO powder was prepared by microwave treatment of ammoniacal and carbonate Sn6O4(OH)4 suspensions. It was shown that the type of the precipitant (aqueous ammonia and sodium carbonate) for Sn(II) hydroxy compound affects the surface properties of the resulting oxide. It is found that SnO powders prepared by homogeneous precipitation of tin(II) hydroxy compound with sodium carbonate, followed by the microwave treatment, have the smaller specific surface area (~0.4 m2 g–1) and contain agglomerates of the larger size (~50 µm) joint together into a “flower.” http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Russian Journal of Applied Chemistry Springer Journals

Synthesis and properties of SnO prepared from ammoniacal and carbonate suspensions of tin(II) hydroxy compound under microwave radiation

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Publisher
Pleiades Publishing
Copyright
Copyright © 2015 by Pleiades Publishing, Ltd.
Subject
Chemistry; Chemistry/Food Science, general; Industrial Chemistry/Chemical Engineering
ISSN
1070-4272
eISSN
1608-3296
D.O.I.
10.1134/S1070427215060312
Publisher site
See Article on Publisher Site

Abstract

SnO powder was prepared by microwave treatment of ammoniacal and carbonate Sn6O4(OH)4 suspensions. It was shown that the type of the precipitant (aqueous ammonia and sodium carbonate) for Sn(II) hydroxy compound affects the surface properties of the resulting oxide. It is found that SnO powders prepared by homogeneous precipitation of tin(II) hydroxy compound with sodium carbonate, followed by the microwave treatment, have the smaller specific surface area (~0.4 m2 g–1) and contain agglomerates of the larger size (~50 µm) joint together into a “flower.”

Journal

Russian Journal of Applied ChemistrySpringer Journals

Published: Sep 30, 2015

References

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