Synthesis and kinetic study of N-(1-methyl-3-phenyl-propane)-phthalimide (NP) by phase-transfer catalysis assisted by ultrasound irradiation

Synthesis and kinetic study of N-(1-methyl-3-phenyl-propane)-phthalimide (NP) by phase-transfer... Synthesis of N-(1-methyl-3-phenyl-propane)-phthalimide (NP) was successfully carried out by reacting the potassium phthalimide (PPK) with 2-bromo-1-phenyl propane by using solid–liquid phase-transfer catalysis under nitrogen atmosphere. The effects of agitation rate, reactant concentrations, solvents, catalysts and temperature on the conversion are investigated in the sequence to find the optimum operating environments for this NP formation. It has been found that agitation speed does not affect the reaction once it exceeds 1000 rpm. The apparent reaction rate was first order for the selected reaction. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Research on Chemical Intermediates Springer Journals

Synthesis and kinetic study of N-(1-methyl-3-phenyl-propane)-phthalimide (NP) by phase-transfer catalysis assisted by ultrasound irradiation

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Publisher
Springer Journals
Copyright
Copyright © 2016 by Springer Science+Business Media Dordrecht
Subject
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
ISSN
0922-6168
eISSN
1568-5675
D.O.I.
10.1007/s11164-016-2505-z
Publisher site
See Article on Publisher Site

Abstract

Synthesis of N-(1-methyl-3-phenyl-propane)-phthalimide (NP) was successfully carried out by reacting the potassium phthalimide (PPK) with 2-bromo-1-phenyl propane by using solid–liquid phase-transfer catalysis under nitrogen atmosphere. The effects of agitation rate, reactant concentrations, solvents, catalysts and temperature on the conversion are investigated in the sequence to find the optimum operating environments for this NP formation. It has been found that agitation speed does not affect the reaction once it exceeds 1000 rpm. The apparent reaction rate was first order for the selected reaction.

Journal

Research on Chemical IntermediatesSpringer Journals

Published: Mar 12, 2016

References

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