In this study, we successfully prepared pure, mono-doped, and Ag, Mg co-doped TiO2 nanoparticles using the sol–gel method, with titanium tetraisopropoxide as the Ti source. The prepared samples were characterized by X-ray powder diffraction (XRD), specific surface area and porosity (BET and BJH) measurement, scanning electron microscopy, transmission electron microscopy, X-ray photoelectron spectroscopy, photoluminescence, and energy dispersive X-ray spectroscopy techniques. The XRD data showed that the prepared nanoparticles had the same crystals structures as the pure TiO2. Also, DRS results indicated that the band gap of co-doped photocatalyst was smaller than that of the monometallic and undoped TiO2 and that there was a shift in the absorption band towards the visible light region. Furthermore, the photocatalytic activity of the prepared catalysts was evaluated by the degradation of C.I. Acid Red 27 in aqueous solution under visible light irradiation. The results showed that Ag (0.08 mol%), Mg (0.2 mol%) co-doped TiO2 had the highest photoactivity among all samples under visible light. It was concluded that co-doping of the Ag and Mg can significantly improve the photocatalytic activity of the prepared photocatalysts, due to the efficient inhibition of the recombination of photogenerated electron–hole pairs. The optimum calcination temperature and time were 450 °C and 3 h, respectively.
Research on Chemical Intermediates – Springer Journals
Published: Apr 14, 2015
It’s your single place to instantly
discover and read the research
that matters to you.
Enjoy affordable access to
over 18 million articles from more than
15,000 peer-reviewed journals.
All for just $49/month
Query the DeepDyve database, plus search all of PubMed and Google Scholar seamlessly
Save any article or search result from DeepDyve, PubMed, and Google Scholar... all in one place.
Get unlimited, online access to over 18 million full-text articles from more than 15,000 scientific journals.
Read from thousands of the leading scholarly journals from SpringerNature, Elsevier, Wiley-Blackwell, Oxford University Press and more.
All the latest content is available, no embargo periods.
“Hi guys, I cannot tell you how much I love this resource. Incredible. I really believe you've hit the nail on the head with this site in regards to solving the research-purchase issue.”Daniel C.
“Whoa! It’s like Spotify but for academic articles.”@Phil_Robichaud
“I must say, @deepdyve is a fabulous solution to the independent researcher's problem of #access to #information.”@deepthiw
“My last article couldn't be possible without the platform @deepdyve that makes journal papers cheaper.”@JoseServera