A tin ion-exchanged bentonite seems to be a rather efficient and highly selective catalyst for Baeyer–Villiger oxidation of 2-heptylcyclopentanone to δ-dodecalactone using aqueous hydrogen peroxide (35 wt%) as a clean oxidant. The bentonite-supported tin catalyst was characterized by IR spectroscopy, X-ray diffraction spectroscopy, and scanning electron microscopy. Methanesulfonic acid and sodium dodecyl sulfate promoted conversion of 2-heptylcyclopentanone to δ-dodecalactone in high (81 %) yield.
Research on Chemical Intermediates – Springer Journals
Published: Jul 30, 2013
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