NiO@CuO@Cu bilayered electrode: two-step electrochemical synthesis supercapacitor properties

NiO@CuO@Cu bilayered electrode: two-step electrochemical synthesis supercapacitor properties Present work deals with a two-step synthesis and electrochemical properties of nickel oxide @copper oxide@copper (NiO@CuO@Cu) bilayered electrode. In the first step, anodization (40 V for 25 min) of Cu foil has been carried out for forming Cu-hydroxide@Cu which when annealed at 300 °C for 1 h produces CuO@Cu. In the second step, Ni-hydroxide is deposited onto CuO@Cu by applying current density of 0.03 A/cm2 for 3 min which when re-annealed at 300 °C for 1 h gives out NiO@CuO@Cu bilayered electrode. Obtained NiO@CuO@Cu bilayered electrode demonstrates separate CuO and NiO phases. The electrochemical properties have obtained using cyclic voltammetry, galvonostatic charge-discharge, and Nyquist plot measurements that reveal an importance of NiO@CuO@Cu as a potential electrode material in the electrochemical supercapacitor application with 58.14, 51.25, and 4.73 F g−1 values in 0.5 M, NaOH, KOH, and Na2SO4 electrolytes, respectively, measured at 2 mVs−1 scan rate. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Journal of Solid State Electrochemistry Springer Journals

NiO@CuO@Cu bilayered electrode: two-step electrochemical synthesis supercapacitor properties

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Publisher
Springer Berlin Heidelberg
Copyright
Copyright © 2017 by Springer-Verlag Berlin Heidelberg
Subject
Chemistry; Physical Chemistry; Electrochemistry; Energy Storage; Characterization and Evaluation of Materials; Analytical Chemistry; Condensed Matter Physics
ISSN
1432-8488
eISSN
1433-0768
D.O.I.
10.1007/s10008-016-3489-8
Publisher site
See Article on Publisher Site

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