New crystalline poly(aniline-co-benzidine)/bentonite microcomposites: synthesis and characterization

New crystalline poly(aniline-co-benzidine)/bentonite microcomposites: synthesis and characterization Polym. Bull. https://doi.org/10.1007/s00289-018-2386-y ORIGINAL PAPER New crystalline poly(aniline‑co‑benzidine)/bentonite microcomposites: synthesis and characterization Ayman S. Al‑Hussaini Received: 22 February 2018 / Revised: 18 April 2018 / Accepted: 23 May 2018 © Springer-Verlag GmbH Germany, part of Springer Nature 2018 Abstract A new series of poly(aniline-co-benzidine)/bentonite microcompos- ites have been fabricated by fivefold molar amounts of aniline to benzidine through utilizing various bentonite quantities by in  situ copolymerization. The obtained outcomes have been justified using spectral and thermal characteristics analyses. Furthermore, the copolymer microcomposites morphology has been investigated uti- lizing SEM and TEM. XRD of the pristine material and microcomposites revealed that they are polycrystalline in their nature. * Ayman S. Al-Hussaini ayman_eldeen@yahoo.com Chemistry Department, Faculty of Science, Port Said University, 23 December Street, Port Said 42521, Egypt 1 3 Polym. Bull. Graphical abstract Keywords Copolymerization · Microcomposites · Bentonite · Crystallinity · Exfoliated composites Introduction Since the mid-1970s, numerous conductive polymers have become widespread research topics [1]. Polyaniline is especially attractive because of its easy synthesis, outstanding environmental stability, high conductivity, novel doping mechanism, promising physi- cal–chemical properties and so far low cost [2, 3]. Consequently, the conductive poly- aniline has been a frontier topic and the most active research areas around the world since the 1980s [4]. In recent http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Polymer Bulletin Springer Journals

New crystalline poly(aniline-co-benzidine)/bentonite microcomposites: synthesis and characterization

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Publisher
Springer Journals
Copyright
Copyright © 2018 by Springer-Verlag GmbH Germany, part of Springer Nature
Subject
Chemistry; Polymer Sciences; Soft and Granular Matter, Complex Fluids and Microfluidics; Characterization and Evaluation of Materials; Physical Chemistry; Organic Chemistry
ISSN
0170-0839
eISSN
1436-2449
D.O.I.
10.1007/s00289-018-2386-y
Publisher site
See Article on Publisher Site

Abstract

Polym. Bull. https://doi.org/10.1007/s00289-018-2386-y ORIGINAL PAPER New crystalline poly(aniline‑co‑benzidine)/bentonite microcomposites: synthesis and characterization Ayman S. Al‑Hussaini Received: 22 February 2018 / Revised: 18 April 2018 / Accepted: 23 May 2018 © Springer-Verlag GmbH Germany, part of Springer Nature 2018 Abstract A new series of poly(aniline-co-benzidine)/bentonite microcompos- ites have been fabricated by fivefold molar amounts of aniline to benzidine through utilizing various bentonite quantities by in  situ copolymerization. The obtained outcomes have been justified using spectral and thermal characteristics analyses. Furthermore, the copolymer microcomposites morphology has been investigated uti- lizing SEM and TEM. XRD of the pristine material and microcomposites revealed that they are polycrystalline in their nature. * Ayman S. Al-Hussaini ayman_eldeen@yahoo.com Chemistry Department, Faculty of Science, Port Said University, 23 December Street, Port Said 42521, Egypt 1 3 Polym. Bull. Graphical abstract Keywords Copolymerization · Microcomposites · Bentonite · Crystallinity · Exfoliated composites Introduction Since the mid-1970s, numerous conductive polymers have become widespread research topics [1]. Polyaniline is especially attractive because of its easy synthesis, outstanding environmental stability, high conductivity, novel doping mechanism, promising physi- cal–chemical properties and so far low cost [2, 3]. Consequently, the conductive poly- aniline has been a frontier topic and the most active research areas around the world since the 1980s [4]. In recent

Journal

Polymer BulletinSpringer Journals

Published: May 31, 2018

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