Various spectroscopic methods and X-ray phase analysis were applied to study the distribution of copper(II) and lead(II) between the solution and the precipitate of (NH4)2Na[Rh(NO2)6]. Promising methods are proposed for fine purification of ammonium sodium hexanitrites of rhodium(III) and iridium(III) to remove contaminants, irrespective of the mechanism of their ingress into crystalline phases.
Russian Journal of Applied Chemistry – Springer Journals
Published: Oct 13, 2004
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