Morphology of polyaniline nanofibers synthesized under different conditions

Morphology of polyaniline nanofibers synthesized under different conditions Polyaniline nanofibers are readily synthesized by bulk polymerization; ammonium per sulphate (APS) is used as oxidizing agent and hydrochloric acid as dopant without any hard or soft templates. A detailed study was conducted on the effect of a variety of synthetic conditions on the size and morphology of the polyaniline nanostructure. These conditions include the concentration of dopant, and the APS-to-aniline and acid-to-aniline molar ratios. The morphology of the nanofibers was confirmed by SEM and TEM. XRD and FT-IR and UV–visible spectroscopy were used for structural characterization of nanofibers. The results showed that not only the microstructure of the polyaniline product, but also other characteristics, for example conductivity, crystallinity, and, more importantly, the efficiency of the process are strongly affected by the synthetic conditions. Research on Chemical Intermediates Springer Journals

Morphology of polyaniline nanofibers synthesized under different conditions

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Springer Netherlands
Copyright © 2013 by Springer Science+Business Media Dordrecht
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
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