Materials characterization part I: contact area of the Berkovich indenter for nanoindentation tests

Materials characterization part I: contact area of the Berkovich indenter for nanoindentation tests This is the first of two papers associated with materials characterization methods based on hardness testing. This paper presents a method to determine the area function of the Berkovich indenter used in nanoindentation hardness tests. The geometry and hence projected area of the indenter is known to affect the force-displacement response of a material during the loading and unloading stages. It is therefore important that the projected area is accurately defined to ensure determination of correct material hardness values. It is shown that values for the projected area determined from numerical methods applied to experimental data differ from values predicted inversely from theory based on the assumption of perfect tip geometry. This difference is attributed principally to a blunting of the tip, presenting as a tip radius. A simulation of the nanoindentation hardness test system is developed using finite element modelling (FEM) methods. Solutions for a range of load indentation curves obtained from experiment with fused silica are determined from best fit analyses using the root mean square error objective function (RMSE). A linear regression method is subsequently developed and used to estimate the area function. A parametric study of simulation and experimental results has been completed to verify the FEM and to assess the influence of varying tip curvature on force-displacement response during the loading and unloading stages and is summarily reported. A new method of analysis for determination of area function is proposed for use with numerical-based simulations, which for the first time, accommodates variation in tip geometry and which is shown to deliver improved agreement with nanoindentation experimental results. The second paper will focus on the study of the tip geometry of the Vickers microindenter. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png The International Journal of Advanced Manufacturing Technology Springer Journals

Materials characterization part I: contact area of the Berkovich indenter for nanoindentation tests

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Publisher
Springer London
Copyright
Copyright © 2017 by Springer-Verlag London
Subject
Engineering; Industrial and Production Engineering; Media Management; Mechanical Engineering; Computer-Aided Engineering (CAD, CAE) and Design
ISSN
0268-3768
eISSN
1433-3015
D.O.I.
10.1007/s00170-017-0115-6
Publisher site
See Article on Publisher Site

Abstract

This is the first of two papers associated with materials characterization methods based on hardness testing. This paper presents a method to determine the area function of the Berkovich indenter used in nanoindentation hardness tests. The geometry and hence projected area of the indenter is known to affect the force-displacement response of a material during the loading and unloading stages. It is therefore important that the projected area is accurately defined to ensure determination of correct material hardness values. It is shown that values for the projected area determined from numerical methods applied to experimental data differ from values predicted inversely from theory based on the assumption of perfect tip geometry. This difference is attributed principally to a blunting of the tip, presenting as a tip radius. A simulation of the nanoindentation hardness test system is developed using finite element modelling (FEM) methods. Solutions for a range of load indentation curves obtained from experiment with fused silica are determined from best fit analyses using the root mean square error objective function (RMSE). A linear regression method is subsequently developed and used to estimate the area function. A parametric study of simulation and experimental results has been completed to verify the FEM and to assess the influence of varying tip curvature on force-displacement response during the loading and unloading stages and is summarily reported. A new method of analysis for determination of area function is proposed for use with numerical-based simulations, which for the first time, accommodates variation in tip geometry and which is shown to deliver improved agreement with nanoindentation experimental results. The second paper will focus on the study of the tip geometry of the Vickers microindenter.

Journal

The International Journal of Advanced Manufacturing TechnologySpringer Journals

Published: Feb 24, 2017

References

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