In situ DRIFTS study on the synthesis of N-alkylmorpholines

In situ DRIFTS study on the synthesis of N-alkylmorpholines In situ diffuse reflectance Fourier-transform infrared spectroscopy was used to perform mechanistic investigation on the synthesis of N-alkylmorpholines from diethylene glycol (DEG), alcohol and ammonia. The results showed that the synthesis of N-alkylmorpholines on a heterogeneous catalyst proceeded along the reaction path between DEG and alkylamine when choosing CuO–NiO/γ-Al2O3 as a suitable catalyst. In addition, the yield of methylmorpholine and ethylmorpholine was 86.4 and 76.6 %, respectively. Research on Chemical Intermediates Springer Journals

In situ DRIFTS study on the synthesis of N-alkylmorpholines

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Springer Netherlands
Copyright © 2012 by Springer Science+Business Media B.V.
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
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