Hydrothermal synthesis and ESR analysis of NiO dendrite and tree-like nanostructures

Hydrothermal synthesis and ESR analysis of NiO dendrite and tree-like nanostructures NiO dendrites and tree-like nanostructures were successfully synthesized by hydrothermal reaction of Ni(NO3)2, ethylenediamine, and thiourea. It was found that achievement of such structures depended on the duration time of the hydrothermal method, the temperature, and the capping agents used. The obtained powder was characterized by X-ray diffraction (XRD) analysis, Fourier-transform infrared spectroscopy, transmission electron microscopy, high-resolution transmission electron microscopy, and electron paramagnetic resonance spectroscopy (ESR). The g value obtained from the paramagnetic resonance signal was g = 2.022, corresponding to Ni2+ ion in NiO. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Research on Chemical Intermediates Springer Journals

Hydrothermal synthesis and ESR analysis of NiO dendrite and tree-like nanostructures

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Publisher
Springer Netherlands
Copyright
Copyright © 2016 by Springer Science+Business Media Dordrecht
Subject
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
ISSN
0922-6168
eISSN
1568-5675
D.O.I.
10.1007/s11164-016-2799-x
Publisher site
See Article on Publisher Site

Abstract

NiO dendrites and tree-like nanostructures were successfully synthesized by hydrothermal reaction of Ni(NO3)2, ethylenediamine, and thiourea. It was found that achievement of such structures depended on the duration time of the hydrothermal method, the temperature, and the capping agents used. The obtained powder was characterized by X-ray diffraction (XRD) analysis, Fourier-transform infrared spectroscopy, transmission electron microscopy, high-resolution transmission electron microscopy, and electron paramagnetic resonance spectroscopy (ESR). The g value obtained from the paramagnetic resonance signal was g = 2.022, corresponding to Ni2+ ion in NiO.

Journal

Research on Chemical IntermediatesSpringer Journals

Published: Nov 1, 2016

References

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