Hydrothermal synthesis and characterization of Nd-doped ZnSe nanoparticles with enhanced visible light photocatalytic activity

Hydrothermal synthesis and characterization of Nd-doped ZnSe nanoparticles with enhanced visible... In the present study, Nd3+-doped ZnSe nanoparticles with variable Nd contents were successfully synthesized via a hydrothermal process using Neodymium (III) chloride hexahydrate as the doping source. X-ray diffraction, UV–Vis diffuse reflectance spectroscopy (DRS), scanning electron microscopy and transmission electron microscopy were used for characterization of the synthesized nanoparticles. It was confirmed by the DRS analysis that both of the undoped and Nd-doped ZnSe samples had significant optical absorption in the visible light range. The photocatalytic performance of as-synthesized nanoparticles was investigated towards the decolorization of C. I. Acid Orange 7 solution under visible light irradiation. Results indicated that the loading of Nd dopant into ZnSe nanoparticles significantly enhanced the photocatalytic activity of pure ZnSe with increasing Nd loading up to 6 mol% (color removal efficiency of 24.31 % for ZnSe and 84.20 % for Nd0.06Zn0.94Se after 120 min of treatment) and then the photocatalytic activity began to decrease. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Research on Chemical Intermediates Springer Journals

Hydrothermal synthesis and characterization of Nd-doped ZnSe nanoparticles with enhanced visible light photocatalytic activity

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Publisher
Springer Netherlands
Copyright
Copyright © 2012 by Springer Science+Business Media Dordrecht
Subject
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
ISSN
0922-6168
eISSN
1568-5675
D.O.I.
10.1007/s11164-012-0977-z
Publisher site
See Article on Publisher Site

Abstract

In the present study, Nd3+-doped ZnSe nanoparticles with variable Nd contents were successfully synthesized via a hydrothermal process using Neodymium (III) chloride hexahydrate as the doping source. X-ray diffraction, UV–Vis diffuse reflectance spectroscopy (DRS), scanning electron microscopy and transmission electron microscopy were used for characterization of the synthesized nanoparticles. It was confirmed by the DRS analysis that both of the undoped and Nd-doped ZnSe samples had significant optical absorption in the visible light range. The photocatalytic performance of as-synthesized nanoparticles was investigated towards the decolorization of C. I. Acid Orange 7 solution under visible light irradiation. Results indicated that the loading of Nd dopant into ZnSe nanoparticles significantly enhanced the photocatalytic activity of pure ZnSe with increasing Nd loading up to 6 mol% (color removal efficiency of 24.31 % for ZnSe and 84.20 % for Nd0.06Zn0.94Se after 120 min of treatment) and then the photocatalytic activity began to decrease.

Journal

Research on Chemical IntermediatesSpringer Journals

Published: Dec 27, 2012

References

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