Formation of Solid Electrolyte Film Structures

Formation of Solid Electrolyte Film Structures Dependence of the effect of highly efficient milling on preparation of dense solid electrolytes in the form of films of chemically deposited zirconium dioxide powder is studied on the example of the system ZrO2 + 8 mol.% Y2O3. Changes in ZrO2 particle morphology and composition occurring during milling affect sintered ceramic properties. During sintering there is inheritance of the powder structure. A reduction in the degree of agglomeration during milling of chemically precipitated powders in a bead mill (to 2 μm) makes it possible to obtain a more compact nanostructure (to 50 nm) during sintering compared with the structure of specimens from powders after milling in a ball mill. Optimum properties are determined for starting powders in order to prepare high quality dense films up to 170 μm thick by pouring on to a moving substrate. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Refractories and Industrial Ceramics Springer Journals

Formation of Solid Electrolyte Film Structures

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Publisher
Springer US
Copyright
Copyright © 2015 by Springer Science+Business Media New York
Subject
Material Science; Characterization and Evaluation of Materials; Materials Science, general; Ceramics, Glass, Composites, Natural Methods
ISSN
1083-4877
eISSN
1573-9139
D.O.I.
10.1007/s11148-015-9737-0
Publisher site
See Article on Publisher Site

Abstract

Dependence of the effect of highly efficient milling on preparation of dense solid electrolytes in the form of films of chemically deposited zirconium dioxide powder is studied on the example of the system ZrO2 + 8 mol.% Y2O3. Changes in ZrO2 particle morphology and composition occurring during milling affect sintered ceramic properties. During sintering there is inheritance of the powder structure. A reduction in the degree of agglomeration during milling of chemically precipitated powders in a bead mill (to 2 μm) makes it possible to obtain a more compact nanostructure (to 50 nm) during sintering compared with the structure of specimens from powders after milling in a ball mill. Optimum properties are determined for starting powders in order to prepare high quality dense films up to 170 μm thick by pouring on to a moving substrate.

Journal

Refractories and Industrial CeramicsSpringer Journals

Published: Feb 11, 2015

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