Formation of Material Prescribed Phase Composition from Refractory Filler Silica Powder Modified with Alkoxide and Sol-Gel Composite

Formation of Material Prescribed Phase Composition from Refractory Filler Silica Powder Modified... Creation of ceramics and refractories with improved physicomechanical properties is possible with use of nanomaterials in their technology. Introduction of SiC nanoparticles into a ceramic material charge by using modified filler powders is proposed. Fillers modified with tetraethoxysilane during grinding leads to powder crystal structure breakdown and SiC mechanochemical synthesis. The amount of β-SiC synthesized in this way depends on the amount of modifying additive. Results are provided for modified filler phase composition before and after heat treatment at 1000°C, and mechanochemically synthesized SiC thermal stability is established. It is shown that sintering of modified electro-corundum worsens with an increase in amount of synthesized silicon carbide nanoparticles. The difference is demonstrated in phase composition formation with heat treatment of a mixture of modified and normal finely ground electrocorundum with a sol-gel binder and firing up to 1600°C. Silicon carbide nanoparticle synthesis does not exceed 3 – 7 % in both cases. Recommendations are given for use of corundum filler with a different amount of modifying additive. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Refractories and Industrial Ceramics Springer Journals

Formation of Material Prescribed Phase Composition from Refractory Filler Silica Powder Modified with Alkoxide and Sol-Gel Composite

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Publisher
Springer Journals
Copyright
Copyright © 2014 by Springer Science+Business Media New York
Subject
Material Science; Characterization and Evaluation of Materials; Materials Science, general; Ceramics, Glass, Composites, Natural Methods
ISSN
1083-4877
eISSN
1573-9139
D.O.I.
10.1007/s11148-014-9697-9
Publisher site
See Article on Publisher Site

Abstract

Creation of ceramics and refractories with improved physicomechanical properties is possible with use of nanomaterials in their technology. Introduction of SiC nanoparticles into a ceramic material charge by using modified filler powders is proposed. Fillers modified with tetraethoxysilane during grinding leads to powder crystal structure breakdown and SiC mechanochemical synthesis. The amount of β-SiC synthesized in this way depends on the amount of modifying additive. Results are provided for modified filler phase composition before and after heat treatment at 1000°C, and mechanochemically synthesized SiC thermal stability is established. It is shown that sintering of modified electro-corundum worsens with an increase in amount of synthesized silicon carbide nanoparticles. The difference is demonstrated in phase composition formation with heat treatment of a mixture of modified and normal finely ground electrocorundum with a sol-gel binder and firing up to 1600°C. Silicon carbide nanoparticle synthesis does not exceed 3 – 7 % in both cases. Recommendations are given for use of corundum filler with a different amount of modifying additive.

Journal

Refractories and Industrial CeramicsSpringer Journals

Published: Sep 23, 2014

References

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