Formation of Compounds in the Ag2O–Sb2O3–MoO3 System on Heating

Formation of Compounds in the Ag2O–Sb2O3–MoO3 System on Heating This paper presents a detailed study of phase formation processes in the AgNO3–Sb2O3–MoO3 system during heating in air. The compositions of the solid-state reaction products have been determined using thermogravimetry and qualitative X-ray diffraction. The results demonstrate that, at a final heat treatment temperature of 1023 K, synthesis yields a range of Ag2–x Sb2–x Mo x O6 compounds with the pyrochlore structure and 0.0 ≤ x ≤ 2.0. The structural parameters of the synthesized phases have been refined by the Rietveld method in space group Fd3̅m and their electrical conductivity has been measured. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Inorganic Materials Springer Journals

Formation of Compounds in the Ag2O–Sb2O3–MoO3 System on Heating

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Publisher
Springer Journals
Copyright
Copyright © 2018 by Pleiades Publishing, Ltd.
Subject
Chemistry; Inorganic Chemistry; Industrial Chemistry/Chemical Engineering; Materials Science, general
ISSN
0020-1685
eISSN
1608-3172
D.O.I.
10.1134/S0020168518030081
Publisher site
See Article on Publisher Site

Abstract

This paper presents a detailed study of phase formation processes in the AgNO3–Sb2O3–MoO3 system during heating in air. The compositions of the solid-state reaction products have been determined using thermogravimetry and qualitative X-ray diffraction. The results demonstrate that, at a final heat treatment temperature of 1023 K, synthesis yields a range of Ag2–x Sb2–x Mo x O6 compounds with the pyrochlore structure and 0.0 ≤ x ≤ 2.0. The structural parameters of the synthesized phases have been refined by the Rietveld method in space group Fd3̅m and their electrical conductivity has been measured.

Journal

Inorganic MaterialsSpringer Journals

Published: Mar 14, 2018

References

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