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Electrochemical Synthesis of 2,5-Dichloroaniline

Electrochemical Synthesis of 2,5-Dichloroaniline A procedure was proposed for electrochemical reduction of 2,5-dichloronitrobenzene to 2,5-dichloroaniline in aqueous-ethanolic solution of sulfuric acid. The procedure for preparing 2,5-dichloroanilinium sulfate was optimized. The influence exerted by the cathode material, nature and amount of the organic solvent, sulfuric acid concentration, and electrolysis temperature on the yield and quality of the target product was discussed. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Russian Journal of Applied Chemistry Springer Journals

Electrochemical Synthesis of 2,5-Dichloroaniline

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References (2)

Publisher
Springer Journals
Copyright
Copyright © 2003 by MAIK “Nauka/Interperiodica”
Subject
Chemistry; Chemistry/Food Science, general
ISSN
1070-4272
eISSN
1608-3296
DOI
10.1023/A:1026350110061
Publisher site
See Article on Publisher Site

Abstract

A procedure was proposed for electrochemical reduction of 2,5-dichloronitrobenzene to 2,5-dichloroaniline in aqueous-ethanolic solution of sulfuric acid. The procedure for preparing 2,5-dichloroanilinium sulfate was optimized. The influence exerted by the cathode material, nature and amount of the organic solvent, sulfuric acid concentration, and electrolysis temperature on the yield and quality of the target product was discussed.

Journal

Russian Journal of Applied Chemistry – Springer Journals

Published: Oct 3, 2004

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