Effect of synthesis parameters on the characteristics of expanded graphite were studied. The starting sample, intercalated graphite, was treated by several methods: thermal shock (400, 1000°C) and programmed heating (400–700°C). The samples were examined by scanning electron microscopy, energy-dispersive spectroscopy, X-ray diffraction analysis, and low-temperature nitrogen adsorption. The programmed-heating method yields better texture characteristics as compared with the thermal shock. The programmed-heating method was used to obtain high-quality expanded graphite with high specific surface area (299 m2 g–1) at a comparatively moderate temperature of 400°C.
Russian Journal of Applied Chemistry – Springer Journals
Published: Feb 9, 2017
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