Effect of Milling and Sintering Temperature of TaC–TaB2 Composite on Lattice Parameter and C/Ta Ratio

Effect of Milling and Sintering Temperature of TaC–TaB2 Composite on Lattice Parameter and C/Ta... The lattice parameter of TaC–TaB2 balk prepared by mechano-chemical and spark plasma sintering (SPS) was investigated by the Nelson–Riley method. In this study, TaC–B4C powder was milled for 3, 6, 9, 12 hours and sintered by spark plasma sintering. The lattice parameter and C/Ta ratio of TaC–TaB2 was calculated by the Nelson–Riley method and the Storms relation. In this research, TaC–B4C powder was reacted and produced TaC–TaB2 composite. Phase formation and powder morphology during milling and sintering were examined using different analysis techniques including XRD and FE-SEM. The lattice parameter of the powders was increased by milling time and sintering temperature. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Refractories and Industrial Ceramics Springer Journals

Effect of Milling and Sintering Temperature of TaC–TaB2 Composite on Lattice Parameter and C/Ta Ratio

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Publisher
Springer US
Copyright
Copyright © 2017 by Springer Science+Business Media New York
Subject
Materials Science; Characterization and Evaluation of Materials; Materials Science, general; Ceramics, Glass, Composites, Natural Materials
ISSN
1083-4877
eISSN
1573-9139
D.O.I.
10.1007/s11148-017-0013-3
Publisher site
See Article on Publisher Site

Abstract

The lattice parameter of TaC–TaB2 balk prepared by mechano-chemical and spark plasma sintering (SPS) was investigated by the Nelson–Riley method. In this study, TaC–B4C powder was milled for 3, 6, 9, 12 hours and sintered by spark plasma sintering. The lattice parameter and C/Ta ratio of TaC–TaB2 was calculated by the Nelson–Riley method and the Storms relation. In this research, TaC–B4C powder was reacted and produced TaC–TaB2 composite. Phase formation and powder morphology during milling and sintering were examined using different analysis techniques including XRD and FE-SEM. The lattice parameter of the powders was increased by milling time and sintering temperature.

Journal

Refractories and Industrial CeramicsSpringer Journals

Published: Mar 29, 2017

References

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