Determination of 2,6-di-tert-butylphenol in Irganox 1425

Determination of 2,6-di-tert-butylphenol in Irganox 1425 An ion suppression reversed phase high performance liquid chromatography method has been developed for the determination of 2,6-di-tert-butylphenol in Irganox 1425. Separation was carried out on a Welch Material Ultimate XB-C18 column (5 μm, 150 mm × 4.6 mm), using methanol–water (0.1 % HClO4) (75/25, v/v) mixture as the mobile phase in an isocratic elution. Detection was performed by UV absorption at a wavelength of 275 nm, and the limit of detection was 0.2 μg/mL. The method presented excellent repeatability and precision with both intra- and inter-day relative standard deviations (RSDs) of less than 2.0 %, as well as satisfactory accuracy with the recovery of 98.7–102.3 %, and therefore can be applied for the quality control analysis of Irganox 1425 industrial product. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Research on Chemical Intermediates Springer Journals

Determination of 2,6-di-tert-butylphenol in Irganox 1425

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Publisher
Springer Netherlands
Copyright
Copyright © 2012 by Springer Science+Business Media B.V.
Subject
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
ISSN
0922-6168
eISSN
1568-5675
D.O.I.
10.1007/s11164-012-0734-3
Publisher site
See Article on Publisher Site

Abstract

An ion suppression reversed phase high performance liquid chromatography method has been developed for the determination of 2,6-di-tert-butylphenol in Irganox 1425. Separation was carried out on a Welch Material Ultimate XB-C18 column (5 μm, 150 mm × 4.6 mm), using methanol–water (0.1 % HClO4) (75/25, v/v) mixture as the mobile phase in an isocratic elution. Detection was performed by UV absorption at a wavelength of 275 nm, and the limit of detection was 0.2 μg/mL. The method presented excellent repeatability and precision with both intra- and inter-day relative standard deviations (RSDs) of less than 2.0 %, as well as satisfactory accuracy with the recovery of 98.7–102.3 %, and therefore can be applied for the quality control analysis of Irganox 1425 industrial product.

Journal

Research on Chemical IntermediatesSpringer Journals

Published: Jul 28, 2012

References

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