Characterization of ZnO–TiO2 and zinc titanate nanoparticles synthesized by hydrothermal process

Characterization of ZnO–TiO2 and zinc titanate nanoparticles synthesized by hydrothermal process Solutions containing zinc nitrate hexahydrate (Zn(NO3)2·6H2O) and potassium titanium oxalate dihydrate (C4K2O9Ti·2H2O) with different molar ratios of Zn:Ti at a pH of 10 were hydrothermally processed at 120, 160, and 200 °C to form ZnO–anatase, ZnO–anatase–rutile and ZnO–rutile nanocomposites. Upon subsequent calcination the precursors at high temperatures, ZnTiO3, Zn2TiO4 , and Zn2Ti3O8 nanoparticles were synthesized. X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), Fourier transform infrared (FTIR) spectroscopy, Raman spectrophotometry, and photoluminescence (PL) spectroscopy revealed the existence of nanocomposites and nanoparticles with strong emission at 386 nm for Zn2TiO4 and Zn2Ti3O8 and at 370 nm for ZnTiO3. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Research on Chemical Intermediates Springer Journals

Characterization of ZnO–TiO2 and zinc titanate nanoparticles synthesized by hydrothermal process

Loading next page...
 
/lp/springer_journal/characterization-of-zno-tio2-and-zinc-titanate-nanoparticles-XAtmsfM1pH
Publisher
Springer Netherlands
Copyright
Copyright © 2016 by Springer Science+Business Media Dordrecht
Subject
Chemistry; Catalysis; Physical Chemistry; Inorganic Chemistry
ISSN
0922-6168
eISSN
1568-5675
D.O.I.
10.1007/s11164-016-2818-y
Publisher site
See Article on Publisher Site

Abstract

Solutions containing zinc nitrate hexahydrate (Zn(NO3)2·6H2O) and potassium titanium oxalate dihydrate (C4K2O9Ti·2H2O) with different molar ratios of Zn:Ti at a pH of 10 were hydrothermally processed at 120, 160, and 200 °C to form ZnO–anatase, ZnO–anatase–rutile and ZnO–rutile nanocomposites. Upon subsequent calcination the precursors at high temperatures, ZnTiO3, Zn2TiO4 , and Zn2Ti3O8 nanoparticles were synthesized. X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), Fourier transform infrared (FTIR) spectroscopy, Raman spectrophotometry, and photoluminescence (PL) spectroscopy revealed the existence of nanocomposites and nanoparticles with strong emission at 386 nm for Zn2TiO4 and Zn2Ti3O8 and at 370 nm for ZnTiO3.

Journal

Research on Chemical IntermediatesSpringer Journals

Published: Nov 28, 2016

References

You’re reading a free preview. Subscribe to read the entire article.


DeepDyve is your
personal research library

It’s your single place to instantly
discover and read the research
that matters to you.

Enjoy affordable access to
over 12 million articles from more than
10,000 peer-reviewed journals.

All for just $49/month

Explore the DeepDyve Library

Unlimited reading

Read as many articles as you need. Full articles with original layout, charts and figures. Read online, from anywhere.

Stay up to date

Keep up with your field with Personalized Recommendations and Follow Journals to get automatic updates.

Organize your research

It’s easy to organize your research with our built-in tools.

Your journals are on DeepDyve

Read from thousands of the leading scholarly journals from SpringerNature, Elsevier, Wiley-Blackwell, Oxford University Press and more.

All the latest content is available, no embargo periods.

See the journals in your area

DeepDyve Freelancer

DeepDyve Pro

Price
FREE
$49/month

$360/year
Save searches from Google Scholar, PubMed
Create lists to organize your research
Export lists, citations
Read DeepDyve articles
Abstract access only
Unlimited access to over
18 million full-text articles
Print
20 pages/month
PDF Discount
20% off