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- Publisher
- Springer Journals
- Copyright
- Copyright © 2009 by Springer Science+Business Media, Inc.
- Subject
- Chemistry; Inorganic Chemistry ; Organic Chemistry; Chemistry/Food Science, general
- ISSN
- 1066-5285
- eISSN
- 1573-9171
- DOI
- 10.1007/s11172-009-0331-9
- Publisher site
- See Article on Publisher Site
Abstract
High molecular weight nitroxyl radicals formed directly in polymerization system (in situ) from N-tert-buiyl-C-phenylnitrone are efficient agents for the chain growth control and allow one to perform synthesis of di- and triblock-copolymers based on a number of vinylic monomers (styrene, methyl methacrylate, N-vinylpyrrolidone, and butyl acrylate) under more mild temperature regimes than their low molecular weight analogs. The macromolecular structures synthesized are characterized by GPC, NMR and IR spectroscopy, and MALDI TOF MS method.
Journal
Russian Chemical Bulletin – Springer Journals
Published: Sep 25, 2010