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Separation of diastereomers of a 1,3-disubstituted tetrahydro-β-carboline by capillary electrophoresis with β-cyclodextrin

Separation of diastereomers of a 1,3-disubstituted tetrahydro-β-carboline by capillary... Capillary zone electrophoresis with β-cyclodextrin as electrolyte additive has been investigated for the separation of the diastereomers of a 1,3-disubstituted tetrahydro-β-carboline. The effects of pH, buffer concentration, β-cyclodextrin concentration and applied voltage on resolution were investigated. This study shows that optimizing the assay conditions leads to maximum chiral separation or resolution. The method enables further research on the quantitative analysis of these compounds. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Chromatographia Springer Journals

Separation of diastereomers of a 1,3-disubstituted tetrahydro-β-carboline by capillary electrophoresis with β-cyclodextrin

Chromatographia , Volume 42 (7) – Apr 1, 1996

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References (13)

Publisher
Springer Journals
Copyright
Copyright © 1996 by Friedr. Vieweg & Sohn Verlagsgesellschaft mbH
Subject
Chemistry; Analytical Chemistry; Organic Chemistry; Biochemistry, general; Plant Sciences; Pharmacy; Measurement Science, Instrumentation
ISSN
0009-5893
eISSN
1612-1112
DOI
10.1007/BF02272127
Publisher site
See Article on Publisher Site

Abstract

Capillary zone electrophoresis with β-cyclodextrin as electrolyte additive has been investigated for the separation of the diastereomers of a 1,3-disubstituted tetrahydro-β-carboline. The effects of pH, buffer concentration, β-cyclodextrin concentration and applied voltage on resolution were investigated. This study shows that optimizing the assay conditions leads to maximum chiral separation or resolution. The method enables further research on the quantitative analysis of these compounds.

Journal

ChromatographiaSpringer Journals

Published: Apr 1, 1996

There are no references for this article.