Self-Propagating High-Temperature Synthesis of Titanium Carbide Powder under Pressure–Shear Conditions

Self-Propagating High-Temperature Synthesis of Titanium Carbide Powder under Pressure–Shear... This paper presents results of an experimental study of the self-propagating high temperature synthesis (SHS) of titanium carbide powder under pressure in combination with high-temperature shear deformation. We have studied the effect of technologically important parameters, primarily that of the pressure and strain rate, on the synthesis process under pressure–shear conditions. The results demonstrate that a shear load applied to an incompletely formed material during synthesis may have a significant effect on the grain size and morphology, as well as on the mutual arrangement of structural constituents throughout the reaction system. Running the technological SHS process under pressure in combination with shear allows for the synthesis of refractory metals and comminution of the reaction products before cooling to room temperature in a single processing cycle. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Inorganic Materials Springer Journals

Self-Propagating High-Temperature Synthesis of Titanium Carbide Powder under Pressure–Shear Conditions

Stolin, A.; Bazhin, P.; Alymov, M.; Mikheev, M.
Inorganic Materials, Volume 54 (6) – Jun 6, 2018
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Publisher
Springer Journals
Copyright
Copyright © 2018 by Pleiades Publishing, Ltd.
Subject
Chemistry; Inorganic Chemistry; Industrial Chemistry/Chemical Engineering; Materials Science, general
ISSN
0020-1685
eISSN
1608-3172
DOI
10.1134/S0020168518060146
Publisher site
See Article on Publisher Site

Abstract

This paper presents results of an experimental study of the self-propagating high temperature synthesis (SHS) of titanium carbide powder under pressure in combination with high-temperature shear deformation. We have studied the effect of technologically important parameters, primarily that of the pressure and strain rate, on the synthesis process under pressure–shear conditions. The results demonstrate that a shear load applied to an incompletely formed material during synthesis may have a significant effect on the grain size and morphology, as well as on the mutual arrangement of structural constituents throughout the reaction system. Running the technological SHS process under pressure in combination with shear allows for the synthesis of refractory metals and comminution of the reaction products before cooling to room temperature in a single processing cycle.

Journal

Inorganic Materials – Springer Journals

Published: Jun 6, 2018

References

  • History and recent developments in SHS
    Merzhanov, A.G.
  • SHS technology
    Merzhanov, A.G.
  • Solid flames–discoveries, concepts, and horizons of cognition
    Merzhanov, A.G.
  • SHS comminution
    Merzhanov, A.G.; Stolin, A.M.; Mazeiliya, A.V.
  • Peculiarities of the production of elongated items from a ceramic material with nanoscale structure by the SHS extrusion method
    Bazhin, P.M.; Stolin, A.M.; Alymov, M.I.; Chizhikov, A.P.
  • Effects of high shearing stress combined with high hydrostatic pressure
    Bridgman, P.W.
  • Movement of substance on Bridgeman anvils at high-pressure in combination with shear strain
    Zhorin, V.A.; Zharov, A.A.; Kazakevich, A.G.; Enikolopyan, N.S.
  • Synthesis of tungsten nanopowders: comparison of milling, SHS, MASHS and milling-induced chemical processes
    Sarah, D.; Sara, A.; Karim, O.
  • Production of nanocrystalline TiB2 powder through self-propagating high temperature synthesis (SHS) of TiO2–H3BO3–Mg mixture
    Saikumar, G.; Asit, K.; Veerabau, R.
  • Cemented carbides from WC powders obtained by the SHS method
    Zaitsev, A.A.; Vershinnikov, V.I.; Konyashin, I.
  • Manufacture of multipurpose composite and ceramic materials in the combustion regime and high-temperature deformation (SHS extrusion)
    Stolin, A.M.; Bazhin, P.M.
  • Influence of heat treatment on the microstructure and properties of Ti2AlC by SHS/PHIP
    Guobing, Y.; Baona, T.; Xiaodong, H.
  • A study on microstructure and porosity of NiTi alloy implants produced by SHS
    Gul, T.; Latif, O.; Mehmet, K.
  • Methods and techniques for measuring rheological properties of SHS materials
    Stolin, A.M.
  • Self-propagating high-temperature synthesis of ultrafine and nanometer-sized TiC particles
    Borovinskaya, I.P.; Ignat’eva, T.I.; Emel’yanova, O.M.; Vershinnikov, V.I.; Semenova, V.N.

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