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Phase Diagram of the AgNO 3 –CsNO 3 System



The phase diagram of the binary AgNO 3 –CsNO 3 system was constructed using differential thermal analysis (DTA) technique in the range 300–700 K. The apparatus is described briefly. The results exhibit a congruently melting compound CsNO 3 ·AgNO 3 ( m.p. =453 K) characterized by two allotropic varieties α and β, an incongruently melting compound AgNO 3 ·CsNO 3 ( m.p. =450 K) with three forms α′, β′ and γ′, two eutectics (16 mol% CsNO 3 , 442 K and 32.5 mol% CsNO 3 , 445 K) and a peritectic (38mol% CsNO 3 , 450 K). The occurrence of the transitions of intermediates was confirmed by X-ray diffraction at variable temperatures. The phase diagram exhibits also two plateaus at 429 K and 435 K corresponding to the phase transitions of CsNO 3 and AgNO 3 , respectively.



Journal of Thermal Analysis and CalorimetrySpringer Journals

Published: Aug 1, 1999

DOI: 10.1023/A:1010188613487

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