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The first binucleating amino-thiophenolate macrocycles with pendant hydroxyethyl groups.Dalton transactions, 27
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E. Barco, A. Kent, E. Yang, D. Hendrickson (2004)
Quantum superposition of high spin states in the single molecule magnet Ni4.Physical review letters, 93 15
We have investigated magnetic properties of a novel macrocyclic chelate Ni(II) complex [Ni3(L)(OAc)2], by means of the static magnetization M and high field frequency tunable electron spin resonance (HF-ESR). Magnetic field B dependencies of M reveal the magnetic ground state with a total spin S $^{\mathit{tot}}_{0}=1$ and a strong antiferromagnetic coupling between three Ni(II) ions. HF-ESR measurements at frequencies ν=80–350 GHz and B up to 15 T yield a magnetic anisotropy gap of the order of 60 GHz (2.9 K) and a g-factor of 2.2. In addition, the modelling reveals a positive single ion anisotropy (D>0) corresponding to an easy plane situation for the Ni3 complex.
Journal of Low Temperature Physics – Springer Journals
Published: Dec 25, 2009
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