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- Publisher
- Springer Journals
- Copyright
- Copyright © 1997 by Chapman and Hall
- Subject
- Materials Science; Materials Science, general; Characterization and Evaluation of Materials; Polymer Sciences; Continuum Mechanics and Mechanics of Materials; Crystallography and Scattering Methods; Classical Mechanics
- ISSN
- 0022-2461
- eISSN
- 1573-4803
- DOI
- 10.1023/A:1018610719598
- Publisher site
- See Article on Publisher Site
Abstract
The design and use of an apparatus intended to cool samples for in-situ Fourier transform infrared (FTIR) spectroscopy study is described. Using liquid nitrogen as the cooling medium, a working sample temperature of −165°C was achieved. The combination of the cooling stage and FTIR spectroscopy allowed us to study the hydrogen bonding in polyurethanes at very low temperatures in-situ. Experimental results in the N-H and carbonyl absorption regions as a function of temperature are compared.
Journal
Journal of Materials Science – Springer Journals
Published: Sep 10, 2004