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- Publisher
- Springer Journals
- Copyright
- Copyright © 2013 by ASM International
- Subject
- Material Science; Characterization and Evaluation of Materials; Tribology, Corrosion and Coatings; Quality Control, Reliability, Safety and Risk; Engineering Design
- ISSN
- 1059-9495
- eISSN
- 1544-1024
- DOI
- 10.1007/s11665-013-0789-3
- Publisher site
- See Article on Publisher Site
Abstract
The microstructure of Ti-Co polycrystals with 1.6 and 3.2 at.% Co has been studied between 690 and 810 °C after long anneals (720-860 h) in the αTi+β(Ti,Co) two-phase area of the Ti-Co phase diagram. It has been observed that depending on the annealing temperature and GB energy, the αTi phase forms either chains of separated lens-like precipitates or continuous uniform layers along β(Ti,Co)/β(Ti,Co) GBs. In other words, β(Ti,Co)/β(Ti,Co)GBs completely or partially wetted by the αTi phase were observed. At 690 °C, slightly above eutectoid temperature T et = 685 °C, the portion of the completely wetted β(Ti,Co)/β(Ti,Co) GBs is 25% for the Ti-1.6 at.% Co alloy and 60% for the Ti-3.2 at.% Co alloy. It increases with increasing temperature and reaches the maximum of 80% for the Ti-1.6 at.% Co alloy at 780 °C and of 75% for the Ti-3.2 at.% Co alloy at 750 °C. At 810 °C, i.e., close to the upper border of the αTi + β(Ti,Co) two-phase area of the Ti-Co phase diagram, the portion of the completely wetted β(Ti,Co)/β(Ti,Co) GBs drops down to 40% for the Ti-1.6 at.% Co alloy and 20% for the Ti-3.2 at.% Co alloy. Thus, it has been observed for the first time, that the portion of grain boundaries completely wetted by the layers of a second solid phase can non-monotonously depend on the temperature.
Journal
Journal of Materials Engineering and Performance – Springer Journals
Published: Nov 26, 2013