Characterization of a laboratory-constructed miniaturized device for fast CE measurements with contactless conductivity, amperometric, and mass spectrometry detection

Characterization of a laboratory-constructed miniaturized device for fast CE measurements with... Monatsh Chem (2017) 148:1661–1665 DOI 10.1007/s00706-017-1978-9 ORIGINAL PAPER Characterization of a laboratory-constructed miniaturized device for fast CE measurements with contactless conductivity, amperometric, and mass spectrometry detection 1 1 2 • • • Andreas Schmidberger Sebastian Piendl Jonas Josef Peter Mark Frank-Michael Matysik Received: 31 January 2017 / Accepted: 3 April 2017 / Published online: 3 July 2017 Springer-Verlag Wien 2017 Abstract In the recent years, attention for fast separation Graphical abstract of all kind of samples in combination with automated systems has increased. On that account we designed and constructed a miniaturized capillary electrophoresis system which can achieve fast separations due to short capillary length and high electric field strength. An integrated and exchangeable autosampler unit which can be loaded with 19 samples at once allowed high-throughput measurements with small sample volumes down to 30 mm . The design of the device enables the implementation of various detectors. The aim of this work was the analytical characterization of this device in combination with mass spectrometry, Keywords Capillary zone electrophoresis  Amino acids amperometric and capacitively coupled contactless con- Mass spectrometry  Amperometric detection ductivity detection. Hydrodynamic and electrokinetic Contactless conductivity detection injections were carried out with different injection parameters. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Monatshefte für Chemie - Chemical Monthly Springer Journals

Characterization of a laboratory-constructed miniaturized device for fast CE measurements with contactless conductivity, amperometric, and mass spectrometry detection

Loading next page...
 
/lp/springer-journals/characterization-of-a-laboratory-constructed-miniaturized-device-for-zH4AyOv3Kk
Publisher
Springer Journals
Copyright
Copyright © 2017 by Springer-Verlag Wien
Subject
Chemistry; Chemistry/Food Science, general; Organic Chemistry; Inorganic Chemistry; Analytical Chemistry; Physical Chemistry; Theoretical and Computational Chemistry
ISSN
0026-9247
eISSN
1434-4475
D.O.I.
10.1007/s00706-017-1978-9
Publisher site
See Article on Publisher Site

Abstract

Monatsh Chem (2017) 148:1661–1665 DOI 10.1007/s00706-017-1978-9 ORIGINAL PAPER Characterization of a laboratory-constructed miniaturized device for fast CE measurements with contactless conductivity, amperometric, and mass spectrometry detection 1 1 2 • • • Andreas Schmidberger Sebastian Piendl Jonas Josef Peter Mark Frank-Michael Matysik Received: 31 January 2017 / Accepted: 3 April 2017 / Published online: 3 July 2017 Springer-Verlag Wien 2017 Abstract In the recent years, attention for fast separation Graphical abstract of all kind of samples in combination with automated systems has increased. On that account we designed and constructed a miniaturized capillary electrophoresis system which can achieve fast separations due to short capillary length and high electric field strength. An integrated and exchangeable autosampler unit which can be loaded with 19 samples at once allowed high-throughput measurements with small sample volumes down to 30 mm . The design of the device enables the implementation of various detectors. The aim of this work was the analytical characterization of this device in combination with mass spectrometry, Keywords Capillary zone electrophoresis  Amino acids amperometric and capacitively coupled contactless con- Mass spectrometry  Amperometric detection ductivity detection. Hydrodynamic and electrokinetic Contactless conductivity detection injections were carried out with different injection parameters.

Journal

Monatshefte für Chemie - Chemical MonthlySpringer Journals

Published: Jul 3, 2017

References

You’re reading a free preview. Subscribe to read the entire article.


DeepDyve is your
personal research library

It’s your single place to instantly
discover and read the research
that matters to you.

Enjoy affordable access to
over 18 million articles from more than
15,000 peer-reviewed journals.

All for just $49/month

Explore the DeepDyve Library

Search

Query the DeepDyve database, plus search all of PubMed and Google Scholar seamlessly

Organize

Save any article or search result from DeepDyve, PubMed, and Google Scholar... all in one place.

Access

Get unlimited, online access to over 18 million full-text articles from more than 15,000 scientific journals.

Your journals are on DeepDyve

Read from thousands of the leading scholarly journals from SpringerNature, Elsevier, Wiley-Blackwell, Oxford University Press and more.

All the latest content is available, no embargo periods.

See the journals in your area

DeepDyve

Freelancer

DeepDyve

Pro

Price

FREE

$49/month
$360/year

Save searches from
Google Scholar,
PubMed

Create lists to
organize your research

Export lists, citations

Read DeepDyve articles

Abstract access only

Unlimited access to over
18 million full-text articles

Print

20 pages / month

PDF Discount

20% off