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The Preparation and Structures of Ph2P(E)OH and Ph2P(E) OP(E) Ph2 (E = S, Se)

The Preparation and Structures of Ph2P(E)OH and Ph2P(E) OP(E) Ph2 (E = S, Se) The preparation and characterization of the title compounds is reported. The selenium compounds have been characterized by x-ray crystallography. Ph2P (Se)OH 1 Pbca a = 6.203(1), b = 16.949(4), c = 22.939(5) Å, Z = 8,1523 observed data, R = 0.033, Rw = 0.038. Ph2P(Se)OP(Se)Ph22 C2/c a = 15.426(4), b = 9.232(3), c = 18.027(5)Å, β = 118.40(2)°, Z = 4, 1446 observed data, R = 0.028, Rw = 0.030. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Main Group Chemistry IOS Press

The Preparation and Structures of Ph2P(E)OH and Ph2P(E) OP(E) Ph2 (E = S, Se)

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References (6)

Publisher
IOS Press
Copyright
Copyright © 1995 by IOS Press, Inc
ISSN
1024-1221
eISSN
1745-1167
DOI
10.1080/13583149512331338345
Publisher site
See Article on Publisher Site

Abstract

The preparation and characterization of the title compounds is reported. The selenium compounds have been characterized by x-ray crystallography. Ph2P (Se)OH 1 Pbca a = 6.203(1), b = 16.949(4), c = 22.939(5) Å, Z = 8,1523 observed data, R = 0.033, Rw = 0.038. Ph2P(Se)OP(Se)Ph22 C2/c a = 15.426(4), b = 9.232(3), c = 18.027(5)Å, β = 118.40(2)°, Z = 4, 1446 observed data, R = 0.028, Rw = 0.030.

Journal

Main Group ChemistryIOS Press

Published: Jan 1, 1995

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