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Structure of s-triphenyltriazine

Structure of s-triphenyltriazine <h2>Acta Crystallographica</h2><h3></h3><h3>0365-110X</h3> <h2>short communications</h2> Volume 12 Part 3 Pages 258-259 March 1959 <h2>Structure of s -triphenyltriazine</h2> E. Giglio and A. Ripamonti Acta Cryst. (1959). 12, 258 On the crystal structure o1 kernite, Na2B407 Department of Chemistry, Brown University, Providence, (Received 30 September 1958 and As part of a program to correlate X-ray and nuclear magnetic resonance data on the structures of oxy-anions, it was found necessary to re-investigate the crystal structure of kernite. The results of this study indicate that the originally proposed space group and structure (Garrido, 1932; Minder, 1935; Amoros, 1945) are in- consistent with the results of nuclear magnetic resonance studies (Blood & Proctor, 1954; Waterman, 1954; Waterman & Volkoff, 1955; ])as, 1957). Synthetic crystals prepared by Dr W.T. Schaller, U.S. Geological Survey, were examined by the Weissen- berg method using Cu Ka and Me Ka radiation. The correct space group was found to be P21/c not P2/c, owing to the presence of a screw axis since there were systematic extinctions of 0/c0 for k ~= 2n. The Lmit-cell dimensions, obtained from zero-layer line photographs of rotations about the a and b axes yielded the following values: a = 7-022, b -= 9.151±0.002, c = http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Acta Crystallographica International Union of Crystallography

Structure of s-triphenyltriazine

Acta Crystallographica , Volume 12 (3): 258 – Mar 10, 1959

Structure of s-triphenyltriazine

Acta Crystallographica , Volume 12 (3): 258 – Mar 10, 1959

Abstract

<h2>Acta Crystallographica</h2><h3></h3><h3>0365-110X</h3> <h2>short communications</h2> Volume 12 Part 3 Pages 258-259 March 1959 <h2>Structure of s -triphenyltriazine</h2> E. Giglio and A. Ripamonti Acta Cryst. (1959). 12, 258 On the crystal structure o1 kernite, Na2B407 Department of Chemistry, Brown University, Providence, (Received 30 September 1958 and As part of a program to correlate X-ray and nuclear magnetic resonance data on the structures of oxy-anions, it was found necessary to re-investigate the crystal structure of kernite. The results of this study indicate that the originally proposed space group and structure (Garrido, 1932; Minder, 1935; Amoros, 1945) are in- consistent with the results of nuclear magnetic resonance studies (Blood & Proctor, 1954; Waterman, 1954; Waterman & Volkoff, 1955; ])as, 1957). Synthetic crystals prepared by Dr W.T. Schaller, U.S. Geological Survey, were examined by the Weissen- berg method using Cu Ka and Me Ka radiation. The correct space group was found to be P21/c not P2/c, owing to the presence of a screw axis since there were systematic extinctions of 0/c0 for k ~= 2n. The Lmit-cell dimensions, obtained from zero-layer line photographs of rotations about the a and b axes yielded the following values: a = 7-022, b -= 9.151±0.002, c =

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Publisher
International Union of Crystallography
Copyright
Copyright (c) 1959 International Union of Crystallography
ISSN
0365-110X
DOI
10.1107/S0365110X59000809
Publisher site
See Article on Publisher Site

Abstract

<h2>Acta Crystallographica</h2><h3></h3><h3>0365-110X</h3> <h2>short communications</h2> Volume 12 Part 3 Pages 258-259 March 1959 <h2>Structure of s -triphenyltriazine</h2> E. Giglio and A. Ripamonti Acta Cryst. (1959). 12, 258 On the crystal structure o1 kernite, Na2B407 Department of Chemistry, Brown University, Providence, (Received 30 September 1958 and As part of a program to correlate X-ray and nuclear magnetic resonance data on the structures of oxy-anions, it was found necessary to re-investigate the crystal structure of kernite. The results of this study indicate that the originally proposed space group and structure (Garrido, 1932; Minder, 1935; Amoros, 1945) are in- consistent with the results of nuclear magnetic resonance studies (Blood & Proctor, 1954; Waterman, 1954; Waterman & Volkoff, 1955; ])as, 1957). Synthetic crystals prepared by Dr W.T. Schaller, U.S. Geological Survey, were examined by the Weissen- berg method using Cu Ka and Me Ka radiation. The correct space group was found to be P21/c not P2/c, owing to the presence of a screw axis since there were systematic extinctions of 0/c0 for k ~= 2n. The Lmit-cell dimensions, obtained from zero-layer line photographs of rotations about the a and b axes yielded the following values: a = 7-022, b -= 9.151±0.002, c =

Journal

Acta CrystallographicaInternational Union of Crystallography

Published: Mar 10, 1959

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