Synthesis of sub-micro-flakes CrSe2 on glass and (110) Si substrates by solvothermal method

Synthesis of sub-micro-flakes CrSe2 on glass and (110) Si substrates by solvothermal method Layered structure MX2 (M = transition metal, X = S, Se and Te) chalcogenides have rich physic properties and potential applications. While it is still a challenge to prepare the chalcogenides by solvothermal method. In this work, we reported a new solution method to prepare CrSe2 sub-micro-flakes on different substrates. The surface morphologies, structures and compositions of the precursor CrSe2(en)1/2 and CrSe2 were investigated by SEM, XRD, thermogravimetric, IR and Raman spectra. The CrSe2 flakes with the sizes of 5–15 µm were obtained on both glass and (110) Si crystalline substrates. The formation mechanism of CrSe2 sub-micro-flakes is suggested. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Journal of Solid State Chemistry Elsevier

Synthesis of sub-micro-flakes CrSe2 on glass and (110) Si substrates by solvothermal method

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Publisher
Elsevier
Copyright
Copyright © 2018 Elsevier Inc.
ISSN
0022-4596
eISSN
1095-726X
D.O.I.
10.1016/j.jssc.2018.02.020
Publisher site
See Article on Publisher Site

Abstract

Layered structure MX2 (M = transition metal, X = S, Se and Te) chalcogenides have rich physic properties and potential applications. While it is still a challenge to prepare the chalcogenides by solvothermal method. In this work, we reported a new solution method to prepare CrSe2 sub-micro-flakes on different substrates. The surface morphologies, structures and compositions of the precursor CrSe2(en)1/2 and CrSe2 were investigated by SEM, XRD, thermogravimetric, IR and Raman spectra. The CrSe2 flakes with the sizes of 5–15 µm were obtained on both glass and (110) Si crystalline substrates. The formation mechanism of CrSe2 sub-micro-flakes is suggested.

Journal

Journal of Solid State ChemistryElsevier

Published: Jun 1, 2018

References

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