Synthesis and sorption properties of bridged polysilsesquioxane microparticles containing 3-mercaptopropyl groups in the surface layer

Synthesis and sorption properties of bridged polysilsesquioxane microparticles containing... Colloids and Surfaces A 538 (2018) 694–702 Contents lists available at ScienceDirect Colloids and Surfaces A journal homepage: www.elsevier.com/locate/colsurfa Research Paper Synthesis and sorption properties of bridged polysilsesquioxane microparticles containing 3-mercaptopropyl groups in the surface layer a, b,c c d Nataliya V. Stolyarchuk , Hristo Kolev , Maria Kanuchova , Radosław Keller , e a,e Miroslava Vaclavikova , Inna V. Melnyk Chuiko Institute of Surface Chemistry, National Academy of Sciences of Ukraine, 17, Generala Naumova str., Kyiv 03164, Ukraine, Institute of Catalysis, Bulgarian Academy of Sciences, 11, Acad. G. Bonchev str., Sofia 1113, Bulgaria, Technical University of Kosice, 9, Letna str., Kosice 04200, Slovak Republic, Maria Curie-Sklodowska University, 3, Maria Curie-Skłodowska sq., Lublin 20-031, Poland, Institute of Geotechnics, Slovak Academy of Sciences, 45, Watsonova str., Kosice 04001, Slovak Republic GR APHICAL A BSTRACT ARTICLE I NFO ABSTRACT Keywords: In this paper the technique of obtaining mercapto-containing spherical particles based on 1,2-bis(triethoxysilyl) Sol-gel method ethane (BTESE) and 3-mercaptopropyltrimethoxysilane (MPTMS) using the modified Stöber method was de- Hybrid materials veloped. The hydrolytic polycondensation reaction of alkoxysilanes was carried out in ethanol solution and Functionalized bridged polysilsesquioxane catalyzed by fluoride ions. The influence of various factors (ratio of reacting components, the amount http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Geoderma Elsevier

Synthesis and sorption properties of bridged polysilsesquioxane microparticles containing 3-mercaptopropyl groups in the surface layer

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Publisher
Elsevier
Copyright
Copyright © 2017 Elsevier B.V.
ISSN
0016-7061
eISSN
1872-6259
D.O.I.
10.1016/j.colsurfa.2017.11.049
Publisher site
See Article on Publisher Site

Abstract

Colloids and Surfaces A 538 (2018) 694–702 Contents lists available at ScienceDirect Colloids and Surfaces A journal homepage: www.elsevier.com/locate/colsurfa Research Paper Synthesis and sorption properties of bridged polysilsesquioxane microparticles containing 3-mercaptopropyl groups in the surface layer a, b,c c d Nataliya V. Stolyarchuk , Hristo Kolev , Maria Kanuchova , Radosław Keller , e a,e Miroslava Vaclavikova , Inna V. Melnyk Chuiko Institute of Surface Chemistry, National Academy of Sciences of Ukraine, 17, Generala Naumova str., Kyiv 03164, Ukraine, Institute of Catalysis, Bulgarian Academy of Sciences, 11, Acad. G. Bonchev str., Sofia 1113, Bulgaria, Technical University of Kosice, 9, Letna str., Kosice 04200, Slovak Republic, Maria Curie-Sklodowska University, 3, Maria Curie-Skłodowska sq., Lublin 20-031, Poland, Institute of Geotechnics, Slovak Academy of Sciences, 45, Watsonova str., Kosice 04001, Slovak Republic GR APHICAL A BSTRACT ARTICLE I NFO ABSTRACT Keywords: In this paper the technique of obtaining mercapto-containing spherical particles based on 1,2-bis(triethoxysilyl) Sol-gel method ethane (BTESE) and 3-mercaptopropyltrimethoxysilane (MPTMS) using the modified Stöber method was de- Hybrid materials veloped. The hydrolytic polycondensation reaction of alkoxysilanes was carried out in ethanol solution and Functionalized bridged polysilsesquioxane catalyzed by fluoride ions. The influence of various factors (ratio of reacting components, the amount

Journal

GeodermaElsevier

Published: Feb 15, 2019

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