J. of Supercritical Fluids 114 (2016) 26–31 Contents lists available at ScienceDirect The Journal of Supercritical Fluids journal homepage: www.elsevier.com/locate/supflu Study of self-association of gradient copolymers in supercritical CO thanks to synchrotron and in-house small-angle X-rays scattering measurements a b b,∗ a,∗ F. Gasc , B. Corso , J. Causse , P. Lacroix-Desmazes Institut Charles Gerhardt—UMR-5253 CNRS, ENSCM, UM, Ingénierie et Architectures Macromoléculaires (IAM), ENSCM, 8 rue de l’Ecole Normale, 34296 Montpellier Cedex 5, France Institut de Chimie Séparative de Marcoule (ICSM), UMR 5257—CEA/CNRS/UM2/ENSCM, Site de Marcoule, Bâtiment 426, 30207 Bagnols sur Cèze, France article info abstract Article history: Speciﬁc comblike gradient copolymers made of metal-complexing CO -phobic units and ﬂuorinated CO - 2 2 Received 23 February 2016 philic units were designed to study their self-association when solubilised in supercritical CO (scCO ). 2 2 Received in revised form 8 April 2016 This paper shows that in-house SAXS measurements on scCO systems are now possible thanks to both Accepted 9 April 2016 high-energy X-rays and speciﬁc high-pressure cell designed with beryllium windows. The copolymer Available online 11 April 2016 system poly(1,1,2,2-tetrahydroperﬂuorodecylacrylate-co-4-(diphenylphosphino)styrene), poly(FDA-co- DPPS) was compared to homopolymer with thiol endgroup poly(FDA)-SH and more classical molecule, Keywords: C F
The Journal of Supercritical Fluids – Elsevier
Published: Aug 1, 2016
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