Rapid precipitation of Mg-doped fluoride-based submicron spheres and evolution study

Rapid precipitation of Mg-doped fluoride-based submicron spheres and evolution study The present study investigates a rapid and template-free precipitation method for syntheses of Mg-doped fluoride based submicron spheres. The precipitates can be obtained less than one minute. The method also reveals the magnesium function in the formation of fluoride-based spherical submicron particles. The morphologies and structure changes of precipitates over time were studied via SEM and TEM. The surface bumps of Mg-doped BaF2 spheres disappeared after 4-h aging. Significant size increases of the particles have been observed. The evolution process during 4-h aging was typically Ostwald ripening. http://www.deepdyve.com/assets/images/DeepDyve-Logo-lg.png Journal of Solid State Chemistry Elsevier

Rapid precipitation of Mg-doped fluoride-based submicron spheres and evolution study

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Publisher
Elsevier
Copyright
Copyright © 2018 Elsevier Inc.
ISSN
0022-4596
eISSN
1095-726X
D.O.I.
10.1016/j.jssc.2018.01.026
Publisher site
See Article on Publisher Site

Abstract

The present study investigates a rapid and template-free precipitation method for syntheses of Mg-doped fluoride based submicron spheres. The precipitates can be obtained less than one minute. The method also reveals the magnesium function in the formation of fluoride-based spherical submicron particles. The morphologies and structure changes of precipitates over time were studied via SEM and TEM. The surface bumps of Mg-doped BaF2 spheres disappeared after 4-h aging. Significant size increases of the particles have been observed. The evolution process during 4-h aging was typically Ostwald ripening.

Journal

Journal of Solid State ChemistryElsevier

Published: Apr 1, 2018

References

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